Toluene → HCID 23693107, Verbindung

HRID 1089641

Reaktionsgleichung

Reaktionsgleichung von HRID 1089641
C(OC)(=O)C1C=CC(C([O-])=O)=CC=1.[K+:14].[C:15]([O:28]CC)(=[O:27])[C:16]1[CH:26]=[CH:25][C:19]([C:20]([O:22][CH2:23][CH3:24])=[O:21])=[CH:18][CH:17]=1.[OH-].[K+].C1(C)C=CC=CC=1>C(O)C>[C:20]([O:22][CH2:23][CH3:24])(=[O:21])[C:19]1[CH:25]=[CH:26][C:16]([C:15]([O-:28])=[O:27])=[CH:17][CH:18]=1.[K+:14]

Komponenten

6

Edukt 4

HCID 1140TolueneHCID 12483Diethyl terephthalateHCID 14797Potassium HydroxideHCID 236837531,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1)

Produkt 1

HCID 23693107HCID 23693107, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

This compound was prepared by the procedure described for potassium monomethyl terephthalate. Typical reagent levels were as follows: 77.0 gm (0.346 mole) of diethyl terephthalate, 19.4 gm of potassium hydroxide, 150 ml of toluene and 100 ml of ethanol.

Aufarbeitung

  1. customThis compound was prepared by the procedure

Quellen und Nachweise

ORD-Eintrag
ord-6fc1ab55849247b0a645d3cb5ff02d94
Quelldatensatz
uspto-grants-1992_01
Patentnummer
US05078907

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