Thionyl Chloride → Monopropyl Terephthaloyl Chloride

HRID 1089643Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1089643
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCC)(=O)[C:15]1C=CC(C([O-])=O)=CC=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH3:15]

Komponenten

5

Edukt 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, VerbindungHCID 23693908Potassium Monopropyl Terephthalate

Produkt 1

HCID 19915522Monopropyl Terephthaloyl Chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monopropyl terephthalate (49.0g, 0.20 mole), thionyl chloride (29.8g, 0.25 mole) and 100 ml of toluene. The product was used without further purification.

Aufarbeitung

  1. customThis compound was prepared by the procedure
  2. customThe product was used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-ac7eb9e4db084883b32afbccc60fb5aa
Quelldatensatz
uspto-grants-1992_01
Patentnummer
US05078907

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