Thionyl Chloride → Monohexyl Terephthaloyl Chloride

HRID 1089648Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1089648
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].C(OCCCCCC)(=O)[C:15]1[CH:23]=[CH:22]C(C([O-])=O)=[CH:17][CH:16]=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:17][CH2:16][CH2:15][CH2:23][CH3:22]

Komponenten

5

Edukt 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, VerbindungHCID 23693907Potassium monohexyl terephthalate

Produkt 1

HCID 19915510Monohexyl Terephthaloyl Chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

This compound was prepared by the method described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monohexyl terephthalate (18.6 g, 0.64 mole), thionyl chloride (9.21 g, 0.774 mole) and 100 ml of toluene. The product was used without further purification.

Aufarbeitung

  1. customThis compound was prepared by the method
  2. customThe product was used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-5ebe672c30364d6da854725a7ce28276
Quelldatensatz
uspto-grants-1992_01
Patentnummer
US05078907

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