4-Amino-2-methylpyridine → HCID 58007539, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[CH:7]=[CH:6][N:5]=[C:4]([CH3:8])[CH:3]=1.[C:9]([C:17](Cl)=[O:18])(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH3:8][C:4]1[CH:3]=[C:2]([NH:1][C:17](=[O:18])[C:9](=[O:16])[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:7]=[CH:6][N:5]=1Komponenten
3
Versuchsvorschrift
In analogy to the procedure described for the synthesis example 41 (step 1), the title compound N-(2-methyl-pyridin-4-yl)-2-oxo-2-phenyl-acetamide (MS m/e: 241.2 [M+H]+) was prepared from 4-amino-2-picoline and benzoylformic acid chloride.
Aufarbeitung
- customIn analogy to the procedure described for the synthesis example 41 (step 1)
Quellen und Nachweise
- ORD-Eintrag
- ord-4aa516d5231449dea7c09880550b060b
- Quelldatensatz
- uspto-grants-2012_03
- Patentnummer
- US08133909B2
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