HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Nitroisophthalic acid → 4-Aminobenzene-1,3-dioic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Nitroisophthalic acid | HCID 3062438 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-Aminobenzene-1,3-dioic acid | HCID 11355852 | — |
Reaktionsschritte
To a solution of 4-nitro isophthalic acid (4 g, 18.95 mmol) in MeOH (200 mL) was added Pd/C (20%) and the mixture was hydrogenated at RT over night. The reaction mixture was filtered through Celite and filtrate concentrated under vacuum to give 4-amino isophthalic acid in 60% as a solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08133998B2 |
| Quelldatensatz | uspto-grants-2012_03 |
| ORD ID | ord-a70aad4b64f84b4ba0494f54b48628cb |
| Quellennotiz | uspto-grants-2012_03 |