2-Acrylamido-2-methyl-1-propanesulfonic acid → Ammonium acryloyldimethyltaurate
Reaktionsgleichung
COCCOCC[N:8](CCOCCOC)CCOCCOC.[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([OH:33])(=[O:32])=[O:31])(=[O:26])[CH:24]=[CH2:25]>>[NH4+:8].[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([O-:33])(=[O:31])=[O:32])(=[O:26])[CH:24]=[CH2:25]Komponenten
3
Versuchsvorschrift
A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.
Aufarbeitung
- customA nitrogen purged 50 ml schlenk flask