HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Myristic Acid → Tetradecanoic acid, cadmium salt (2:1)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Myristic Acid | HCID 11005 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Cadmium Nitrate | HCID 25154 | — |
| Edukt | Sodium Myristate | HCID 23693095 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Tetradecanoic acid, cadmium salt (2:1) | HCID 66290 | — |
Reaktionsschritte
Cadmium nitrate (5 mmol) was dissolved in anhydrous methanol (50 mL). A sodium-myristate solution was prepared by dissolving sodium hydroxide (15 mmol) and myristic acid (15 mmol) in anhydrous methanol (500 mL). Then the cadmium-nitrate solution was added dropwise (one drop per second) into the sodium-myristate solution with vigorous stirring. The resulting white precipitate was washed with methanol three times, and then dried at ˜60° C. under vacuum overnight.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08137457B2 |
| Quelldatensatz | uspto-grants-2012_03 |
| ORD ID | ord-f36c17c4339b4b88b5e836b296c9a53d |
| Quellennotiz | uspto-grants-2012_03 |