HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(Difluoromethoxy)benzyl alcohol → 1-(2-Butenyl)-7-(4-difluoromethoxybenzyloxy)-2,3-dimethylpyrrolo[2,3-d]pyridazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(Difluoromethoxy)benzyl alcohol | HCID 2736996 | — |
| Edukt | 1-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53719624 | — |
| Produkt | 1-(2-Butenyl)-7-(4-difluoromethoxybenzyloxy)-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53682881 | 37,8% |
Reaktionsschritte
The title compound (cis/trans=21/79) was prepared as a white powder in 37.8% yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine (cis/trans=20/80) and 4-difluoromethoxybenzyl alcohol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06063782 |
| Quelldatensatz | uspto-grants-2000_05 |
| ORD ID | ord-55dac3f409764200bde777084ec3c99f |
| Quellennotiz | uspto-grants-2000_05 |