Allyl bromide → Methyl 3-formyl-4,5-dimethyl-1-(2-propenyl)pyrrole-2-carboxylate

Reaktionsgleichung

[CH:1]([C:3]1[C:7]([CH3:8])=[C:6]([CH3:9])[NH:5][C:4]=1[C:10]([O:12][CH3:13])=[O:11])=[O:2].Br[CH2:15][CH:16]=[CH2:17]>>[CH:1]([C:3]1[C:7]([CH3:8])=[C:6]([CH3:9])[N:5]([CH2:17][CH:16]=[CH2:15])[C:4]=1[C:10]([O:12][CH3:13])=[O:11])=[O:2]

Komponenten

Edukt 2

HCID 7841Allyl bromide

HCID 10773740Methyl 3-formyl-4,5-dimethyl-1H-pyrrole-2-carboxylate

Produkt 1

HCID 18785652Methyl 3-formyl-4,5-dimethyl-1-(2-propenyl)pyrrole-2-carboxylate

Versuchsvorschrift

The title compound was prepared as a yellow solid in 95.1% yeild in a similar procedure to that described in Referential Example 9 by using methyl 3-formyl-4,5-dimethylpyrrole-2-carboxylate and 3-bromo-1-propene.

Quellen und Nachweise

ORD-Eintrag: ord-e43b5c51161f4672873ddeab43377c58
Quelldatensatz: uspto-grants-2000_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06063782

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