HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 4'-n-Nonyloxybiphenyl-4-carboxylic acid chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 4'-(Nonyloxy)[1,1'-biphenyl]-4-carboxylic acid | HCID 3620263 | — |
| Produkt | 4'-n-Nonyloxybiphenyl-4-carboxylic acid chloride | HCID 12080273 | — |
Reaktionsschritte
After 1.2 g of 4'-n-nonyloxybiphenyl-4-carboxylic acid was heated together with an excess amount of thionyl chloride for 6 hours under a reflux condition, unaltered thionyl chloride was distilled off to obtain 1.25 g of 4'-n-nonyloxybiphenyl-4-carboxylic acid chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05320776 |
| Quelldatensatz | uspto-grants-1994_06 |
| ORD ID | ord-b75ec5e9a4644b7d97f746bc7a0b9d13 |
| Quellennotiz | uspto-grants-1994_06 |