HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glyoxylic Acid → (+-)-4-Hydroxymandelic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glyoxylic Acid | HCID 760 | — |
| Edukt | Phenol | HCID 996 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | (+-)-4-Hydroxymandelic acid | HCID 328 | — |
Reaktionsschritte
condensing glyoxylic acid with phenol at a temperature of 15°-80° C. in the absence of a strong mineral base and in the presence of a tertiary amine, said tertiary amine being insoluble or slightly soluble in water and being liquid at ambient temperature, and said glyoxylic acid being in aqueous solution at a concentration greater than 50% by weight, to produce parahydroxymandelic acid, and
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04978784 |
| Quelldatensatz | uspto-grants-1990_12 |
| ORD ID | ord-a74aed0fa6184b7ea8d9cd0ab3154f0f |
| Quellennotiz | uspto-grants-1990_12 |