HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hexamethylenediamine → N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine]
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hexamethylenediamine | HCID 16402 | — |
| Edukt | 1,2-Epoxytetradecane | HCID 18604 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] | HCID 21332395 | — |
Reaktionsschritte
In a manner similar to that of Example 1, condensation of 1-tetradecene oxide (91.8 g.) and hexamethylenediamine (25 g.) and recrystallization of the resulting product (71 g., m.p. 118°-121° C.) from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] (I: R = CH3 (CH2)11, R' = H, X = (CH2)6, Z = H) (55.3 g., m.p. 122°-126° C.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04119668 |
| Quelldatensatz | uspto-grants-1978_10 |
| ORD ID | ord-d984b79a673644ef93ab7c2fe01e94be |
| Quellennotiz | uspto-grants-1978_10 |