N-Methylaniline → N-Methylacetanilide
Reaktionsgleichung
[CH:1]([O:4]P(O)OC(C)C)(C)[CH3:2].[CH3:11][NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH3:11][N:12]([C:1](=[O:4])[CH3:2])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1Komponenten
3
Versuchsvorschrift
Example 34 was repeated, except that 0.05 mole of phosphorous diisopropyl ester was used in place of phosphorous monoethyl ester and 0.05 mole of N-methylaniline was used in place of aniline, to obtain N-methylacetanilide, yield 53% based on N-methylaniline.
Quellen und Nachweise
- ORD-Eintrag
- ord-8a38a4fb241b4e6fab67ba63bed738da
- Quelldatensatz
- uspto-grants-1978_10
- Patentnummer
- US04120853
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