HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Benzyl-1H-benzo[d]imidazol-2(3H)-one → 4-Benzyl-2-(1-benzyl-2,3-dihydro-benzimidazol-2-on-3-yl-methyl)-morpholine hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Benzyl-1H-benzo[d]imidazol-2(3H)-one | HCID 736505 | — |
| Edukt | 4-Benzyl-2-(chloromethyl)morpholine | HCID 2801562 | — |
| Produkt | 4-Benzyl-2-(1-benzyl-2,3-dihydro-benzimidazol-2-on-3-yl-methyl)-morpholine hydrochloride | HCID 70601713 | 44,4% |
Reaktionsschritte
The condensation of 0.1 mol of 1-benzyl-2,3-dihydrobenzimidazol-2-one and 0.1 mol of 2-chloromethyl-4-benzyl-morpholine is carried out in accordance with the procedure of Example 1. 20 g of 4-benzyl-2-(1-benzyl-2,3-dihydro-benzimidazol-2-on-3-yl-methyl)-morpholine hydrochloride are obtained, m.p. 196° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04122175 |
| Quelldatensatz | uspto-grants-1978_10 |
| ORD ID | ord-93684b07e9dd42a9b59344751e532e15 |
| Quellennotiz | uspto-grants-1978_10 |