HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 4-Iodo-3-methylbenzoate → Methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 4-Iodo-3-methylbenzoate | HCID 231757 | — |
| Edukt | 5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid | HCID 19694676 | — |
| Produkt | Methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate | HCID 19694687 | 53% |
Reaktionsschritte
Following the basic procedure of Example 7(f), by reacting 2.8 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid with 1.84 g (6.7 mmol) of methyl 3-methyl-4-iodobenzoate, 1.37 g (53%) of methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate was obtained in the form of a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05723499 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-7949d567ab7542a8990b7bcf17a467de |
| Quellennotiz | uspto-grants-1998_03 |