1-Iodopropane → methyl N-propyl-4-iodo-2-pyrrolecarboxylate

HRID 1139

Reaktionsgleichung

Reaktionsgleichung von HRID 1139
[I:1][C:2]1[CH:3]=[C:4]([C:7]([O:9][CH3:10])=[O:8])[NH:5][CH:6]=1.I[CH2:12][CH2:13][CH3:14]>>[CH2:12]([N:5]1[CH:6]=[C:2]([I:1])[CH:3]=[C:4]1[C:7]([O:9][CH3:10])=[O:8])[CH2:13][CH3:14]

Komponenten

3

Edukt 2

HCID 336431-IodopropaneHCID 11673249methyl 4-iodo-1H-pyrrole-2-carboxylate

Produkt 1

HCID 19694682methyl N-propyl-4-iodo-2-pyrrolecarboxylateAusbeute 64,7 %

Versuchsvorschrift

Following the basic procedure of Example 7(d), by reacting 1.96 g (7.8 mmol) of methyl 4-iodo-2-pyrrolecarboxylate with 940 μl (9.6 mmol) of 3-iodopropane, 1.48 g (64%) of methyl N-propyl-4-iodo-2-pyrrolecarboxylate was obtained in the form of a slightly yellow oil.

Quellen und Nachweise

ORD-Eintrag
ord-5fa351dbe3ea452bbf01e7f31dec9368
Quelldatensatz
uspto-grants-1998_03
Patentnummer
US05723499

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