4-(2-(Diethylamino)ethoxy)aniline → HCID 178418791, Verbindung
Reaktionsgleichung
[CH2:1]([N:3]([CH2:14][CH3:15])[CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([NH2:13])=[CH:9][CH:8]=1)[CH3:2].[CH3:16][C:17]1[CH:25]=[CH:24][CH:23]=[C:22]2[C:18]=1[C:19](=[CH:27]O)[C:20](=[O:26])[NH:21]2>>[CH2:14]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]([NH:13][CH:27]=[C:19]2[C:18]3[C:22](=[CH:23][CH:24]=[CH:25][C:17]=3[CH3:16])[NH:21][C:20]2=[O:26])=[CH:11][CH:12]=1)[CH3:15]Komponenten
3
Versuchsvorschrift
In a manner similar to that describe in Example 231, 4-(2-diethylamino-ethoxy)-phenylamine (713 mg, 1.2 equiv.) and 4-methyl-3-hydroxymethylene-1,3-dihydro-indol-2-one (500 mg, 2.86 mmol, 1 equiv.) are reacted to give the named compound as a yellow solid (237 mg, 23%).
Aufarbeitung
- customare reacted
Quellen und Nachweise
- ORD-Eintrag
- ord-e20d14176b5048e8a6ea5c9122514271