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Sodium Hydroxide → 2-Amino-7-(p-chloro-benzoyl)-6,7,8,9-tetrahydro-5H-pyrazino[2,3-d]azepine

HRID 1153752
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 1153752
[Cl:1][C:2]1[CH:18]=[CH:17][C:5]([C:6]([N:8]2[CH2:14][CH2:13][C:12](=O)[C:11](=O)[CH2:10][CH2:9]2)=[O:7])=[CH:4][CH:3]=1.ClC1C=CC(C(N2CCCC(=O)CC2)=O)=CC=1.[Se](=O)=O.Br.Br.[NH2:41][CH2:42][C:43]([NH2:45])=[NH:44].[OH-].[Na+]>O1CCOCC1.O.CO.C(OCC)(=O)C>[NH2:45][C:43]1[CH:42]=[N:41][C:12]2[CH2:13][CH2:14][N:8]([C:6](=[O:7])[C:5]3[CH:17]=[CH:18][C:2]([Cl:1])=[CH:3][CH:4]=3)[CH2:9][CH2:10][C:11]=2[N:44]=1
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Komponenten

9

Edukt 5

HCID 14798Sodium HydroxideHCID 24007Selenium DioxideHCID 16211382Aminoacetamidine DihydrobromideHCID 204364131-(4-Chloro-benzoyl)-hexahydroazepine-4-oneHCID 204364431-(4-Chloro-benzoyl)-hexahydroazepine-4,5-dione

Produkt 1

HCID 13037042
2-Amino-7-(p-chloro-benzoyl)-6,7,8,9-tetrahydro-5H-pyrazino[2,3-d]azepine

Reagenzien, Katalysatoren, Lösungsmittel 3

HCID 887MethanolLösungsmittelHCID 8857Ethyl AcetateLösungsmittelHCID 218864351,4-Dioxane--water (1/1)Lösungsmittel

Versuchsvorschrift

53 mg (0.2 mol) of a mixture of 1-(4-chloro-benzoyl)-hexahydroazepine-4,5-dione and 1-(4-chloro-benzoyl)-hexhydroazepine-3,4-dione [prepared from 1-(4-chloro-benzoyl)-hexahydroazepine-4-one by selenium dioxide oxidation in dioxane/water] and 47 gm (0.2 mol) of 2-amino-acetamidine dihydrobromide were dissolved in 700 ml of methanol, and 200 ml of 2N sodium hydroxide were added dropwise to the solution at 5° C. The mixture was stirred at room temperature for one hour, then concentrated by evaporation and then, after addition of more sodium hydroxide, extracted with chloroform. The dried extract solution was concentrated by evaporation and chromatographed on silicagel with ethyl acetate/methanol (10:1) as the mobile phase. The crystals obtained thereby were digested with ethyl acetate and suction-filtered.

Aufarbeitung

  1. concentrationconcentrated by evaporation
  2. additionafter addition of more sodium hydroxide
  3. extractionextracted with chloroform
  4. extractionThe dried extract solution
  5. concentrationwas concentrated by evaporation
  6. customchromatographed on silicagel with ethyl acetate/methanol (10:1) as the mobile phase
  7. customThe crystals obtained
  8. filtrationsuction-filtered

Quellen und Nachweise

ORD-Eintrag
ord-f5c7b7b1ec0c4d1bb7260ba5004bd7b9
Quelldatensatz
uspto-grants-1984_12
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US04486433

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