Hydrochloric Acid → HCID 178479216, Verbindung

HRID 1154119Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1154119
C([NH:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 178474793HCID 178474793, Verbindung

Produkt 1

HCID 178479216HCID 178479216, Verbindung

Versuchsvorschrift

A mixture of 1-(3-acetamidopropyl)-1H-tetrazole-5-thiol (85 g) and 6N hydrochloric acid (1 l) was refluxed for 75 minutes under stirring. The reaction mixture was concentrated in vacuo and precipitates were collected by filtration and washed with hexane and diethyl ether to give 1-(3-aminopropyl)-1H-tetrazole-5-thiol hydrochloride (67.15 g).

Aufarbeitung

  1. temperaturewas refluxed for 75 minutes
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customprecipitates
  4. filtrationwere collected by filtration
  5. washwashed with hexane and diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-e626872f8af34a81917dbcb23313e739
Quelldatensatz
uspto-grants-1984_12
Patentnummer
US04487767

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