Sulfuric Acid → Octyl 3-mercaptopropionate

HRID 1154514

Reaktionsgleichung

Reaktionsgleichung von HRID 1154514
C(OC)(=O)C=C.[C:7]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])(=[O:10])[CH:8]=[CH2:9].O[S:21](O)(=O)=O>>[CH2:12]([O:11][C:7](=[O:10])[CH2:8][CH2:9][SH:21])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Komponenten

4

Edukt 3

HCID 1118Sulfuric Acid2×HCID 7294Methyl AcrylateHCID 17258Octyl acrylate

Produkt 1

HCID 89128Octyl 3-mercaptopropionateAusbeute 80 %

Versuchsvorschrift

The procedure was as described in Example 1 but in place of methyl acrylate there were employed 184 grams of octyl acrylate and first there were added 250 ml of dilute H2SO4 (4N) and the later 300 ml of dilute H2SO4. After the fractional distillation there were isolated 174.5 grams (corresponding to a yield of 80%) of 3-mercaptopropionic acid octyl ester.

Aufarbeitung

  1. distillationAfter the fractional distillation there

Quellen und Nachweise

ORD-Eintrag
ord-40168e2812b449e38aa362c27a0deb73
Quelldatensatz
uspto-grants-1984_12
Patentnummer
US04490307

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