Dimethyl Sulfoxide → HCID 20434109, Verbindung

HRID 1154616

Reaktionsgleichung

Reaktionsgleichung von HRID 1154616
O.CO[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]([CH:12]=[O:13])=[O:11].[CH3:14][CH:15]([NH2:25])[CH2:16][C:17]1[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=1.[CH3:26]S(C)=O>>[CH3:14][CH:15]([N:25]=[C:12]([O:13][CH3:26])[C:10]([C:5]1[CH:4]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:11])[CH2:16][C:17]1[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=1

Komponenten

4

Edukt 3

HCID 679Dimethyl Sulfoxide2×HCID 31721(+-)-p-MethoxyamphetamineHCID 204341102-Methoxyphenylglyoxal hydrate

Produkt 1

HCID 20434109HCID 20434109, Verbindung

Versuchsvorschrift

2.9 g of 2-methoxyphenylglyoxal hydrate (crude oil) are dissolved in 6 ml of dimethylsulfoxide, and 2 g of α-methyl-4-methoxyphenethylamine are added thereto. The mixture is treated in the same manner as described in Example 1-(2), whereby a solution of α-(α-methyl-4-methoxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.

Aufarbeitung

  1. additionThe mixture is treated in the same manner

Quellen und Nachweise

ORD-Eintrag
ord-0932d662c2e9447a9a8418898ede9ca9
Quelldatensatz
uspto-grants-1984_12
Patentnummer
US04490392

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