Zirconium(IV) propoxide → HCID 86738105, Verbindung

HRID 1155180

Reaktionsgleichung

Reaktionsgleichung von HRID 1155180
C[Si]([O:5][P:6]([CH2:13][CH2:14][CH2:15][CH2:16][C:17]([O:19][CH2:20][CH3:21])=[O:18])(=[O:12])[O:7][Si](C)(C)C)(C)C.[O-]CCC.[Zr+4:26].[O-]CCC.[O-]CCC.[O-]CCC>>[Zr:26].[C:17]([CH2:16][CH2:15][CH2:14][CH2:13][P:6](=[O:5])([O-:12])[O-:7])([O:19][CH2:20][CH3:21])=[O:18]

Komponenten

3

Edukt 2

HCID 90139Zirconium(IV) propoxideHCID 20562960HCID 20562960, Verbindung

Produkt 1

HCID 86738105HCID 86738105, Verbindung

Versuchsvorschrift

To a reaction flask under an inert atmosphere was added 3.13 g of bis-trimethylsilyl-4-carboethoxybutylphosphonate. To the flask was slowly added 1.44 g of zirconium propoxide. After the first few drops were added, a gelatinous product was formed. Agitation was continued during the remainder of the addition.

Aufarbeitung

  1. additionAfter the first few drops were added
  2. customa gelatinous product was formed
  3. additionAgitation was continued during the remainder of the addition

Quellen und Nachweise

ORD-Eintrag
ord-45ed4196492f405b81404d672065348d
Quelldatensatz
uspto-grants-1981_11
Patentnummer
US04299943

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