4-Fluorobenzoyl chloride → 1-(4-Fluorobenzoylamino)-2-(2-methylphenyl)ethane
Reaktionsgleichung
[NH2:1][CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH3:10].[F:11][C:12]1[CH:20]=[CH:19][C:15]([C:16](Cl)=[O:17])=[CH:14][CH:13]=1>>[F:11][C:12]1[CH:20]=[CH:19][C:15]([C:16]([NH:1][CH2:2][CH2:3][C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=2[CH3:10])=[O:17])=[CH:14][CH:13]=1Komponenten
3
Versuchsvorschrift
1-Amino-2-(2-methylphenyl)ethane was reacted with 4-fluorobenzoyl chloride in the same way as in step (a) of Example 1 to afford 1-(4-fluorobenzoylamino)-2-(2-methylphenyl)ethane as colorless needles having a melting point of 82° to 83° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-664993288dc9440389d86bd15832ef3f
- Quelldatensatz
- uspto-grants-1982_06
- Patentnummer
- US04337256
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