Ethyl 1-bromocyclobutanecarboxylate → 6-[(2,2,3,3-tetramethylcyclopropyl)amino]-5-thia-7-azaspiro[3.4]oct-6-en-8-one

HRID 1158005

Reaktionsgleichung

Reaktionsgleichung von HRID 1158005
[CH3:1][C:2]1([CH3:11])[C:4]([CH3:6])([CH3:5])[CH:3]1[NH:7][C:8]([NH2:10])=[S:9].Br[C:13]1([C:17](OCC)=[O:18])[CH2:16][CH2:15][CH2:14]1>>[CH3:1][C:2]1([CH3:11])[C:4]([CH3:5])([CH3:6])[CH:3]1[NH:7][C:8]1[S:9][C:13]2([C:17](=[O:18])[N:10]=1)[CH2:16][CH2:15][CH2:14]2

Komponenten

3

Edukt 2

HCID 97595Ethyl 1-bromocyclobutanecarboxylateHCID 79006986N-(2,2,3,3-tetramethylcyclopropyl)thiourea

Produkt 1

HCID 1784283516-[(2,2,3,3-tetramethylcyclopropyl)amino]-5-thia-7-azaspiro[3.4]oct-6-en-8-one

Versuchsvorschrift

Synthesis was performed from N-(2,2,3,3-tetramethylcyclopropyl)thiourea and ethyl 1-bromocyclobutanecarboxylate according to Method D.

Aufarbeitung

  1. customSynthesis

Quellen und Nachweise

ORD-Eintrag
ord-4c9297568c31493eaf7a109b0fa37dcb
Quelldatensatz
uspto-grants-2010_10
Patentnummer
US07807700B2

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