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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1158191Erstellt: 25. Oktober 2026

1,1'-Biphenyl, 3-nitro- → 3-Aminobiphenyl

https://huagongshe.com/reaction/1158191

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,1'-Biphenyl, 3-nitro-HCID 16450—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
Produkt3-AminobiphenylHCID 1671777,1%

Reaktionsschritte

3-nitrobiphenyl (500 mg, 2.5 mmol) and 10% palladium on carbon (267 mg, 2.5 mmol) were dissolved in methanol (1 mL) and purged with nitrogen and placed under an atmosphere of hydrogen overnight. The reaction mixture was filtered and evaporated to yield 326 mg of the desired amine, which was used directly in Example 12.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07807713B2
Quelldatensatzuspto-grants-2010_10
ORD IDord-fb8eac53c5df4318868e93e72310194f
Quellennotizuspto-grants-2010_10