HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-2-methylpropane → 5-Bromo-2-isobutoxybenzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 5-Bromo-2-hydroxybenzonitrile | HCID 2757014 | — |
| Katalysator | Tetrabutylammonium Bromide | HCID 74236 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 5-Bromo-2-isobutoxybenzonitrile | HCID 66585134 | — |
Reaktionsschritte
5-Bromo-2-hydroxybenzonitrile, isobutyl bromide, and potassium carbonate were heated at 80° C. in DMF in the presence of tetra-n-butylammonium bromide to obtain 5-bromo-2-isobutoxybenzonitrile. F: 254, 256.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07820700B2 |
| Quelldatensatz | uspto-grants-2010_10 |
| ORD ID | ord-b4b0ecc83bbf4e49890fadf070de03a2 |
| Quellennotiz | uspto-grants-2010_10 |