HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentylamine → Cyclopentylthiourea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentylamine | HCID 2906 | — |
| Edukt | Fmoc isothiocyanate | HCID 4154759 | — |
| Produkt | Cyclopentylthiourea | HCID 736945 | — |
Reaktionsschritte
Cyclopentyl-thiourea was prepared following procedure D using cyclopentyl amine (2.4 g, 28 mmol), and Fmoc-isothiocyanate (5.6 g, 20 mmol). Purification (Silica gel, ethyl acetate/hexane 1:1, 100%) provided the product (1.6 g) as white a solid. LCMS m/z: 145 (M+1)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07820704B2 |
| Quelldatensatz | uspto-grants-2010_10 |
| ORD ID | ord-91638c55f14d4de7ba3afd55bb9c1334 |
| Quellennotiz | uspto-grants-2010_10 |