Thionyl Chloride → 2-[(Phenylmethyl)thio]benzoyl chloride

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Thionyl Chloride	HCID 24386	—
Edukt	2-(Benzylsulfanyl)benzoic acid	HCID 264182	—
Lösungsmittel	Benzene	HCID 241	—
Produkt	2-[(Phenylmethyl)thio]benzoyl chloride	HCID 20067340	94,1%

Reaktionsschritte

A suspension of 100 g of 2-[(phenylmethyl)thio]benzoic acid and 97.6 g of thionyl chloride in 800 ml of benzene was refluxed for about three hours then evaporated to dryness under vacuum. The residue was triturated with hexane to yield 101.2 g of 2-[(phenylmethyl)thio]benzoyl chloride, m.p. 113° to 116° C.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04906282
Quelldatensatz	uspto-grants-1990_03
ORD ID	ord-6fc63a9e303d43e2bf6ca3d5569fc421
Quellennotiz	uspto-grants-1990_03