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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1167601Erstellt: 26. Oktober 2026

2,3-Dihydrobenzo(b)furan-5-carboxylic acid → HCID 12985421, Verbindung

https://huagongshe.com/reaction/1167601

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,3-Dihydrobenzo(b)furan-5-carboxylic acidHCID 676583—
Edukt6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepineHCID 11030760—
LösungsmittelDiethyl EtherHCID 3283—
ProduktHCID 12985421HCID 12985421—

Reaktionsschritte

Prepared from 2,3-dihydro-benzofuran-5-carboxylic acid (0.328 g, 2 mmol) and 6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepine (0.398 g, 2 mmol) in a manner essentially identical to that of Example 1. The title compound was obtained as an off-white solid, m.p. 188° C., upon recrystallization from diethyl ether.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06620807B1
Quelldatensatzuspto-grants-2003_09
ORD IDord-7e0f7c5ba55f435f9ef9813b3924f07a
Quellennotizuspto-grants-2003_09