HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Stannous Chloride → 2-Amino-5-fluorobenzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Stannous Chloride | HCID 24479 | — |
| Edukt | 5-Fluoro-2-nitrobenzonitrile | HCID 3756467 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Produkt | 2-Amino-5-fluorobenzonitrile | HCID 2737704 | — |
Reaktionsschritte
The title compound was synthesized from commercially available 2-nitro-5-fluorobenzenecarbonitrile via reduction with SnCl2 in concentrated HCl as previously described in the following reference which is herein incorporated by reference in its entirety for all purposes as if fully set forth herein: Hunziker, F. et al. Eur. J. Med. Chem., Chim. Ther. 1981, 16(5), 391. GC/MS m/z: 136.1 (M+, 100%), Rt 8.87 minutes.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07825132B2 |
| Quelldatensatz | uspto-grants-2010_11 |
| ORD ID | ord-01cbccf3425e409f9d5ffa2a1318af5c |
| Quellennotiz | uspto-grants-2010_11 |