HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Chlorobenzaldehyde → HCID 67373502, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Chlorobenzaldehyde | HCID 11477 | — |
| Edukt | 3-Chlorophenylacetic acid | HCID 15879 | — |
| Edukt | Cyclohexanecarboxaldehyde | HCID 16275 | — |
| Edukt | Cyclohexyl isocyanide | HCID 79129 | — |
| Edukt | Methoxyphenylacetic acid | HCID 107202 | — |
| Edukt | Cyclopentyl Isocyanide | HCID 2734784 | — |
| Edukt | 2-(2-Benzyl-6-chloro-5-fluoro-benzoimidazol-1-yl)-2,N-dicyclohexyl-acetamide | HCID 67373623 | — |
| Produkt | HCID 67373502 | HCID 67373502 | — |
Reaktionsschritte
The title compound was prepared in analogy to Example 1, replacing (2-amino-4,5-difluoro-phenyl)-carbamic acid tert-butyl ester with (2-amino-4-chloro-5-fluoro-phenyl)-carbamic acid tert-butyl ester (([CAS RN 579474-50-3]), Example 47), cyclohexanecarbaldehyde with 3-chlorobenzaldehyde ([CAS RN 587-04-2]), (3-chloro-phenyl)-acetic acid with DL-α-methoxyphenylacetic acid ([CAS RN 7021-09-2]) and cyclohexyl isocyanide with cyclopentyl isocyanide ([CAS RN 68498-54-4]). MS (ISP): 526.2 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07825258B2 |
| Quelldatensatz | uspto-grants-2010_11 |
| ORD ID | ord-2b0d2eaf6c4e4d158c8cef5a29fa8bc7 |
| Quellennotiz | uspto-grants-2010_11 |