Hexane → HCID 57562627, Verbindung

HRID 1172427Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1172427
[NH2:1][C:2]1[N:7]=[C:6]([C:8]([O:10][CH3:11])=[O:9])[CH:5]=[C:4]([Br:12])[CH:3]=1.[C:13]([N:21]=[C:22]=[S:23])(=[O:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.CCCCCC>O1CCCC1>[C:13]([NH:21][C:22](=[S:23])[NH:1][C:2]1[N:7]=[C:6]([C:8]([O:10][CH3:11])=[O:9])[CH:5]=[C:4]([Br:12])[CH:3]=1)(=[O:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Komponenten

5

Edukt 3

HCID 8058HexaneHCID 68284Benzoyl isothiocyanateHCID 29919299Methyl 6-amino-4-bromopyridine-2-carboxylate

Produkt 1

HCID 57562627HCID 57562627, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8028TetrahydrofuranLösungsmittel

Versuchsvorschrift

2.74 g of methyl 6-amino-4-bromopyridine-2-carboxylate was dissolved in 15 ml of tetrahydrofuran and 1.63 ml of benzoyl isothiocyanate was added thereto, followed by stirring at room temperature for 13 hours. To the reaction mixture was added 40 ml of hexane. The resulting solid was filtered and washed with hexane. The obtained solid was dried in vacuo to give the title compound.

Aufarbeitung

  1. filtrationThe resulting solid was filtered
  2. washwashed with hexane
  3. customThe obtained solid was dried in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-3ed8026681ef4d92b94a658b2e7ad497
Quelldatensatz
uspto-grants-2010_11
Patentnummer
US07834018B2

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