HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1H-imidazole-2-carbaldehyde → 1-(1H-Imidazol-2-ylmethyl)-5-phenoxy-1,2,3,4-tetrahydro-quinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1H-imidazole-2-carbaldehyde | HCID 24955 | — |
| Edukt | 5-Phenoxy-1,2,3,4-tetrahydroquinoline | HCID 487547 | — |
| Edukt | Sodium cyanoborohydride | HCID 5003444 | — |
| Katalysator | Zincchloride | HCID 3007855 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 1-(1H-Imidazol-2-ylmethyl)-5-phenoxy-1,2,3,4-tetrahydro-quinoline | HCID 24786231 | — |
Reaktionsschritte
Prepared analogously to Example 1, from 5-phenoxy-1,2,3,4-tetrahydro-quinoline, imidazole-2-carboxaldehyde, zinc chloride and sodium cyanoborohydride in methanol. MS (ISP): 306.3 ([M+H]+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07834044B2 |
| Quelldatensatz | uspto-grants-2010_11 |
| ORD ID | ord-a086ec077fea473b88ffcff308ab65b2 |
| Quellennotiz | uspto-grants-2010_11 |