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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1173911Erstellt: 27. Oktober 2026

1-(Hydroxymethyl)isoquinoline → Isoquinoline-1-carbaldehyde

https://huagongshe.com/reaction/1173911

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-(Hydroxymethyl)isoquinolineHCID 2776247—
KatalysatorHCID 178418406HCID 178418406—
LösungsmittelChloroformHCID 6212—
ProduktIsoquinoline-1-carbaldehydeHCID 26530685,1%

Reaktionsschritte

Isoquinolin-1-yl-methanol (123.7 mg) was dissolved in chloroform (6.2 ml) and then added with manganese dioxide (chemically processed product) (1.24 g), followed by stirring at room temperature for 30 minutes. The reaction solution was filtrated through Celite and the solvent was then distilled off. The residue was dried under vacuum, thereby obtaining the subject compound (103.9 mg) as a brown solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07833991B2
Quelldatensatzuspto-grants-2010_11
ORD IDord-b1e070c7986146688b54b66074608f16
Quellennotizuspto-grants-2010_11