1,1'-Carbonyldiimidazole → HCID 73004887, Verbindung
Reaktionsgleichung
[CH3:1][N:2]1[CH:9]2[CH:5]([N:6]([C:10]3[CH:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=3)[CH2:7][CH2:8]2)[CH2:4][CH2:3]1.[C:17]([N:24]1[CH:28]=[CH:27]N=[CH:25]1)(N1C=CN=C1)=[O:18].[Cl:29][C:30]1[CH:35]=[CH:34][C:33]([CH:36]2CCNC[CH2:37]2)=[CH:32][CH:31]=1>>[CH3:1][N:2]1[CH:9]2[CH:5]([N:6]([C:10]3[CH:15]=[CH:14][C:13]([NH:16][C:17]([N:24]4[CH2:25][CH2:37][CH:36]([C:33]5[CH:34]=[CH:35][C:30]([Cl:29])=[CH:31][CH:32]=5)[CH2:27][CH2:28]4)=[O:18])=[CH:12][CH:11]=3)[CH2:7][CH2:8]2)[CH2:4][CH2:3]1Komponenten
4
Versuchsvorschrift
4-(4-Methylhexahydropyrrolo[3,2-b]pyrrol-1-yl)phenylamine was reacted by method A with carbonyldiimidazole and finally with 4-(4-chlorophenyl)-piperidine. The product with the molecular weight of 439.01 (C25H31ClN4O); MS (ESI): 439 (M+H+) was obtained in this way.
Aufarbeitung
- customMS (ESI): 439 (M+H+) was obtained in this way