HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Phenoxybenzoic acid → n-{2-[(2-Dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-3-phenoxy-benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Phenoxybenzoic acid | HCID 19539 | — |
| Edukt | N2-(2-Dimethylamino-ethyl)-N2-methyl-benzothiazole-2,6-diamine | HCID 55226563 | — |
| Produkt | n-{2-[(2-Dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-3-phenoxy-benzamide | HCID 57771758 | — |
Reaktionsschritte
The title compound is prepared by following General Method A, using 3-phenoxy-benzoic acid (0.22 g, 1.04 mmol), and N*2*-(2-dimethylamino-ethyl)-N*2*-methyl-benzothiazole-2,6-diamine (0.20 g, 0.80 mmol) to afford an off-white solid (0.19 g, 53%). LC/MS: Retention time=4.45 nm in; (m/z): calcd for C25H2(N4O2S (M+H)+: 447.6; found: 447.3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07838543B2 |
| Quelldatensatz | uspto-grants-2010_11 |
| ORD ID | ord-8ec71a69e9324abe86eeb9dbc601afe3 |
| Quellennotiz | uspto-grants-2010_11 |