HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1175201Erstellt: 24. Oktober 2026
Potassium Carbonate → (E)-3-Chloro-N-methyl-N-(1-naphthylmethyl)-2-propen-1-amine
https://huagongshe.com/de/reaction/1175201
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | (E)-1,3-Dichloropropene | HCID 24726 | — |
| Edukt | N-Methyl-N-naphthylmethylamine | HCID 84474 | — |
| Lösungsmittel | Methyl Ethyl Ketone | HCID 6569 | — |
| Produkt | (E)-3-Chloro-N-methyl-N-(1-naphthylmethyl)-2-propen-1-amine | HCID 9834733 | — |
Reaktionsschritte
30 g (0.175 mol) N-methyl-1-naphthalene methanamine, 100 ml MEK and 29 g (0.210 mol, 1.2 eq.) potassium carbonate are introduced into a reactor, the mixture is heated to 50° C. and 22.4 g (0.202 mol, 1.1 eq.) of (1E)-1,3-dichloro-1-propene added dropwise.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07838704B2 |
|---|
| Quelldatensatz | uspto-grants-2010_11 |
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| ORD ID | ord-449e0bb65a6b42839560eb577a526773 |
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| Quellennotiz | uspto-grants-2010_11 |
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