Benzoic acid, 2-hydroxy-4-methyl-, methyl ester → HCID 68503596, Verbindung
Reaktionsgleichung
[OH:1][C:2]1[CH:11]=[C:10]([CH3:12])[CH:9]=[CH:8][C:3]=1[C:4]([O:6][CH3:7])=[O:5].Cl[CH2:14][CH2:15][CH2:16][O:17][CH3:18]>>[CH3:18][O:17][CH2:16][CH2:15][CH2:14][O:1][C:2]1[CH:11]=[C:10]([CH3:12])[CH:9]=[CH:8][C:3]=1[C:4]([O:6][CH3:7])=[O:5]Komponenten
3
Versuchsvorschrift
Analogously to Method F, 103.7 g of methyl 2-hydroxy-4-methylbenzoate are reacted with 95.8 g of 1-chloro-3-methoxypropane. The title compound is obtained as slightly beige oil. Rf=0.27 (1:2 EtOAc-heptane); Rt=4.22.
Quellen und Nachweise
- ORD-Eintrag
- ord-ed745fd6fc284536b8792e3992e4640f
- Quelldatensatz
- uspto-grants-2010_11
- Patentnummer
- US07842688B2
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