1-Chloro-3-methoxypropane → 1-Ethoxy-2-(3-methoxypropoxy)-4-methylbenzene
Reaktionsgleichung
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH3:10])=[CH:6][C:5]=1[OH:11])[CH3:2].Cl[CH2:13][CH2:14][CH2:15][O:16][CH3:17]>>[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH3:10])=[CH:6][C:5]=1[O:11][CH2:13][CH2:14][CH2:15][O:16][CH3:17])[CH3:2]Komponenten
3
Versuchsvorschrift
Analogously to Method F, 5.05 g of 2-ethoxy-5-methylphenol and 4.03 g of 1-chloro-3-methoxypropane are reacted. The title compound is obtained as a slightly orange oil. Rf=0.32 (1:4 EtOAc-heptane); Rt=4.60
Quellen und Nachweise
- ORD-Eintrag
- ord-e8f831e06a64461f841a0442eed89817
- Quelldatensatz
- uspto-grants-2010_11
- Patentnummer
- US07842688B2
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