HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethamivan → Methyl-phenyl-carbamic Acid 4-diethylcarbamoyl-2-methoxy-phenyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethamivan | HCID 9363 | — |
| Edukt | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Produkt | Methyl-phenyl-carbamic Acid 4-diethylcarbamoyl-2-methoxy-phenyl Ester | HCID 69519834 | — |
Reaktionsschritte
The title product was prepared from N,N-diethyl-4-hydroxy-3-methoxy-benzamide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (58%, colorless oil). HPLC-MS: m/z=357.1 (M+1); Rt: 3.64 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07279470B2 |
| Quelldatensatz | uspto-grants-2007_10 |
| ORD ID | ord-b926100beef34922845287d820e3c1cd |
| Quellennotiz | uspto-grants-2007_10 |