Potassium Hydroxide → HCID 69472579, Verbindung

HRID 1180392Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1180392
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=2)[O:9][CH:10]([CH2:15][CH:16]([CH3:18])[CH3:17])[C:11]([O:13]C)=[O:12])=[CH:4][CH:3]=1.[OH-].[K+:26]>>[K+:26].[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=2)[O:9][CH:10]([CH2:15][CH:16]([CH3:18])[CH3:17])[C:11]([O-:13])=[O:12])=[CH:6][CH:7]=1

Komponenten

3

Edukt 2

HCID 14797Potassium HydroxideHCID 69473468Methyl 2-[(4-bromophenyl)(pyridin-2-yl)methoxy]-4-methylpentanoate

Produkt 1

HCID 69472579HCID 69472579, Verbindung

Versuchsvorschrift

Using the same protocol as described in example 17, step 5, methyl 2-[(4-bromophenyl)(pyridin-2-yl)methoxy]-4-methylpentanoate from step 2 (623 mg, 1.59 mmol) was hydrolysed with potassium hydroxide. The solid residue obtained was used as such in the next step.

Aufarbeitung

  1. customThe solid residue obtained

Quellen und Nachweise

ORD-Eintrag
ord-b46738a55dc445ac98279b252b12ae06
Quelldatensatz
uspto-grants-2007_10
Patentnummer
US07279478B2

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