1-Naphthaldehyde → 1-Naphthaldehyde (3-isobutyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)hydrazone
Reaktionsgleichung
[NH:1]([C:3]1[N:8]([CH2:9][CH:10]([CH3:12])[CH3:11])[C:7](=[O:13])[NH:6][C:5](=[O:14])[CH:4]=1)[NH2:2].[C:15]1([CH:25]=O)[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH:18]=[CH:17][CH:16]=1>CO>[CH2:9]([N:8]1[C:3]([NH:1][N:2]=[CH:25][C:15]2[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[CH:18]=[CH:17][CH:16]=2)=[CH:4][C:5](=[O:14])[NH:6][C:7]1=[O:13])[CH:10]([CH3:11])[CH3:12]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
6-hydrazino-1-isobutylpyrimidine-2,4(1H,3H)-dione (1.8 g) was dissolved in warm methanol (90 ml) and treated with 1-naphthaldehyde (1.5 g). After 24 hours, the precipitated solid was filtered and dried to give the subtitle compound (3.03 g).