Dibenzofuran → 2-Iododibenzofuran

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

In a 500 mL three-neck flask was put a suspension of 8.4 g (50 mmol) of dibenzofuran, 6.2 g (25 mmol) of iodine, 5.7 g (25 mmol) of orthoperiodic acid, 150 mL of glacial acetic acid, 30 mL of water, and 500 μL of sulfuric acid, and the suspension was heated and stirred at 60° C. for 4.5 hours to cause a reaction.

Herkunft & Nachweise