HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
m-Chloroperbenzoic acid → 2-Benzenesulfinyl-6-bromo-pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | m-Chloroperbenzoic acid | HCID 70297 | — |
| Edukt | 2-Bromo-6-phenylsulfanylpyridine | HCID 824591 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2-Benzenesulfinyl-6-bromo-pyridine | HCID 86679095 | — |
Reaktionsschritte
2-Bromo-6-phenylsulfanyl-pyridine (0.5323 g, 2 mmol) was dissolved in CH2Cl2 (20 mL) and m-chloroperbenzoic acid (0.345 g, 2 mmol) was added. The reaction was stirred at room temperature overnight then submitted to aqueous workup and purification on silica gel to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08664220B2 |
| Quelldatensatz | uspto-grants-2014_03 |
| ORD ID | ord-26914c45d55841a4a736b549738cd277 |
| Quellennotiz | uspto-grants-2014_03 |