3-Amino-2-hydroxybenzonitrile → Dihydro-8-cyano-2H-1,4-benzoxazine-2-methanamine

HRID 1184359

Reaktionsgleichung

Reaktionsgleichung von HRID 1184359
F[C:2]1[C:11]2[O:10][CH:9]([CH2:12][NH2:13])[CH2:8][NH:7][C:6]=2[CH:5]=[CH:4][CH:3]=1.[NH2:14][C:15]1C=CC=C(C#N)C=1O>>[C:15]([C:2]1[C:11]2[O:10][CH:9]([CH2:12][NH2:13])[CH2:8][NH:7][C:6]=2[CH:5]=[CH:4][CH:3]=1)#[N:14]

Komponenten

3

Edukt 2

HCID 124686813-Amino-2-hydroxybenzonitrileHCID 67497870Dihydro-8-fluoro-2H-1,4-benzoxazine-2-methanamine

Produkt 1

HCID 67497003Dihydro-8-cyano-2H-1,4-benzoxazine-2-methanamine

Versuchsvorschrift

This compound is obtained using the same reaction sequence and the same experimental conditions as those used for the synthesis of intermediate 2b but replacing 2-amino-6-fluorophenol with 2-amino-6-cyanophenol. The title compound of formula (2f) is obtained.

Aufarbeitung

  1. customThis compound is obtained

Quellen und Nachweise

ORD-Eintrag
ord-f59af44eaafe4455970022d0d05fc476
Quelldatensatz
uspto-grants-2014_03
Patentnummer
US08669250B2

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