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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 11860Erstellt: 25. Oktober 2026

Diethylamine → (2S)-2-amino-5-(((tert-butoxy)carbonyl)amino)pentanoic acid

https://huagongshe.com/reaction/11860

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDiethylamineHCID 8021—
EduktFmoc-Orn(Boc)-OHHCID 2756114—
LösungsmittelDimethylformamideHCID 6228—
Produkt(2S)-2-amino-5-(((tert-butoxy)carbonyl)amino)pentanoic acidHCID 6993436210%

Reaktionsschritte

The compound obtained in Example 23-1 (250.8 mg) was dissolved in DMF (5 ml). After the addition of diethylamine. (0.5 ml), the mixture was stirred for 2 hours at room temperature. After the reaction, the solvent was removed by distillation under reduced pressure and the residue was dried under vacuum to obtain the title compound (269.1 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07098215B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-4dc70e910fce4c9ba040b32abaa97152
Quellennotizuspto-grants-2006_08