HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethylamine → (2S)-2-amino-5-(((tert-butoxy)carbonyl)amino)pentanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethylamine | HCID 8021 | — |
| Edukt | Fmoc-Orn(Boc)-OH | HCID 2756114 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | (2S)-2-amino-5-(((tert-butoxy)carbonyl)amino)pentanoic acid | HCID 6993436 | 210% |
Reaktionsschritte
The compound obtained in Example 23-1 (250.8 mg) was dissolved in DMF (5 ml). After the addition of diethylamine. (0.5 ml), the mixture was stirred for 2 hours at room temperature. After the reaction, the solvent was removed by distillation under reduced pressure and the residue was dried under vacuum to obtain the title compound (269.1 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07098215B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-4dc70e910fce4c9ba040b32abaa97152 |
| Quellennotiz | uspto-grants-2006_08 |