N-tert-Butoxycarbonyl-L-aspartic acid beta-benzyl ester → HCID 66874810, Verbindung
Reaktionsgleichung
[ClH:1].Cl.[CH2:3]([O:10][C:11](=[O:19])[CH2:12][C@@H:13]([NH2:18])[CH2:14][N:15]([CH3:17])[CH3:16])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.C(OC(=O)C[C@@H](C(O)=O)NC(OC(C)(C)C)=O)C1C=CC=CC=1>>[ClH:1].[ClH:1].[CH2:3]([O:10][C:11](=[O:19])[CH2:12][C@H:13]([NH2:18])[CH2:14][N:15]([CH3:16])[CH3:17])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1Komponenten
3
Versuchsvorschrift
(S)-3-Amino-4-dimethylamino-butyric acid benzyl ester dihydrochloride was prepared in analogy with (R)-3-amino-4-dimethylamino-butyric acid benzyl ester dihydrochloride (intermediate 1), starting from Boc-L-aspartic acid 4-benzyl ester.
Quellen und Nachweise
- ORD-Eintrag
- ord-eadca96b69bf47f5a123de8886b87a22
- Quelldatensatz
- uspto-grants-2014_03