1-(4-Bromo-3-methylphenyl)ethanone → (R)-2-methyl-propane-2-sulfinic acid [1-(4-bromo-3-methyl-phenyl)ethylidene]-amide

HRID 1191884

Reaktionsgleichung

Reaktionsgleichung von HRID 1191884
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=O)[CH3:9])=[CH:4][C:3]=1[CH3:11].[CH3:12][C:13]([S@:16]([NH2:18])=[O:17])([CH3:15])[CH3:14].C1(C2(CC(O)(C)C)OC(=O)N([C@H](C3C=CC(C4C=CN(C)C(=O)C=4)=CC=3)C)CC2)CC1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[N:18][S@@:16]([C:13]([CH3:15])([CH3:14])[CH3:12])=[O:17])[CH3:9])=[CH:4][C:3]=1[CH3:11]

Komponenten

4

Edukt 3

HCID 3471241-(4-Bromo-3-methylphenyl)ethanoneHCID 10964479tert-Butylsulfinamide, (R)-(+)-HCID 596356736-cyclopropyl-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(1-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenyl)ethyl)-1,3-oxazinan-2-one

Produkt 1

HCID 86649415(R)-2-methyl-propane-2-sulfinic acid [1-(4-bromo-3-methyl-phenyl)ethylidene]-amide

Versuchsvorschrift

The title compound was prepared from 1-(4-bromo-3-methyl-phenyl)-ethanone and (R)-2-methyl-2-propanesulfinamide following a procedure analogous to that described in Step 1 of Intermediate 1. Mass spectrum (ESI+): m/z=316/318 (Br) [M+H]+.

Quellen und Nachweise

ORD-Eintrag
ord-f54cd309031b4477922e394b44d07078
Quelldatensatz
uspto-grants-2014_03
Patentnummer
US08680093B2

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