HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 5-[(3,5-Dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Produkt | 5-[(3,5-Dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxamide | HCID 46932424 | — |
Reaktionsschritte
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and ammonia (0.24 mL, 0.5 M in THF, 0.12 mmol). The title compound was obtained as a solid (4.5 mg, 12.8% yield). MS m/z: 347.80, 349.80 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08680139B2 |
| Quelldatensatz | uspto-grants-2014_03 |
| ORD ID | ord-ebf4a7045c1c4370807cd7bd5beefe52 |
| Quellennotiz | uspto-grants-2014_03 |