HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Nitromethane → (E)-6-nitrohex-5-enal
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Nitromethane | HCID 6375 | — |
| Edukt | Pentanal, 5,5-dimethoxy- | HCID 170903 | — |
| Lösungsmittel | Ethyl acetate hexane | HCID 21226206 | — |
| Produkt | (E)-6-nitrohex-5-enal | HCID 57516560 | 66% |
Reaktionsschritte
Prepared according to the general procedure A from nitromethane 112a (80 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (1.51 g, 66% yield) after silica gel chromatography (EtOAc/Hexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08680335B2 |
| Quelldatensatz | uspto-grants-2014_03 |
| ORD ID | ord-4a9714f50b60466a8e0da7bc31c3558b |
| Quellennotiz | uspto-grants-2014_03 |